A video illustrating a typical practical magnification range of a scanning electron microscope designed for biological specimens. Hitachi ex36005 excavator set of pdf manuals download. Uw images were acquired on the hitachi w filament s3400n vp. Pdf hydrogels are an important class of biomaterials with exceptional promise in biomedical applications 1,2. Remanufactured to oem spec, we can install it, warrant it, and even train your users. This scope is beautiful and clean and was well maintained. The boise state center for materials characterization was established by the idaho state board of education in august 2006 to provide a stateoftheart characterization facility in order to attract more students into science and engineering careers, to improve science and engineering education at.
A bse detector allows tv rate scanning and high resolution imaging. Hitachi s3400n vpsem operation instructions feb, 2014. This well equipped system offers users enhanced performance and capabilities including. Hitachi model s3400n variablepressure sem specifications. Enter your complete name, cmrf user code, date, the starting clock time, and the starting beam time into the record book. The scanning electron microscope is an ideal tool in which to demonstrate this effect on small areas of samples. If you extract this to downloads, desktop or other folders under the user folder this will cause extraction errors that can corrupt the install. General operating instructions for hitachi s4800 high. Opening the chamber to load specimens this may also be done later using the software 1. Hitachi s 3400n ii this variable pressure sem with a tungsten filament is capable of imaging and analysis of pristine materials. Composed of fine to mediumgrained silicon dioxide, st. Screenshots for hitachi ex100, ex100m excavator service manual pdf.
Electron backscatter diffraction ebsd with an hitachi s3400n sem at shizuoka university japan using a 20 kv accelerating voltage, 10. Using microxray fluorescence, the hitachi s3400 n scanning electron. The s 3400n has new electron optics, turbomolecular pumping, a new detector, enhanced sample handling and analysis and improved signal processing and display to ensure high quality images can be obtained from even the most difficult specimens quickly. It is especially suitable for imaging biological and geological specimens. Scanning electron microscopy was carried out with a hitachi s3400n vpsem and temperature. Hitachi s3400n central microscopy research facility. Can we use sem hitachi s3400n for imaging tio2 nanotubes. The morphology of the prepared email protected and the spatial distribution of fe within the polymer beads were observed by scanning electron microscopy sem, hitachi s3400n ii, hitachi, japan. Hitachi s3400n scanning electron microscope hebei north. Hitachi vpsem s3400n the s 3400n offers advances in automation including full filament saturation and no touch objective aperture alignment. For additional assistance, please contact the facility manager. However, due to continuous efforts being made to improve and update the product s, hitachi shall not be liable for any technical or editorial errors or omissions contained in this document, or for any damage, direct or indirect, from discrepancies. Hitachi s3400n vp the hitachi 3400n vpsem is a scanning electron microscope with tungsten filament allowing accelerating voltages up to 30kv. Specimens were observed using a hitachi s 3400n scanning electron microscope hitachi, tokyo, japan operated at an accelerating voltage of 15 kv.
Hitachi vpsem s3400n national metallurgical laboratory. Back to equipment list hitachi s3400 variable pressure sem description the hitachi scanning electron microscope is a variable pressure sem that can image non conductive samples at higher chamber. Oct 30, 2019 the hitachi s3500n variable pressure scanning electron microscope sem. The s3400n main unit from hitachi instruction manual.
Find the user manual and the help you need for the products you own at manualsonline. Hitachi man 3400n scanning electron microscope electron. S3400n scanning electron microscope hitachi science. Using the hitachi ion milling system im4000 su3500 1. The su3500 utilizes a new, more robust condenser lens abating field of view or focus. Instruction manual for model s3400n scanning electron microscope users operationmaintenance edition please read through this manual carefully before using the instrument. The new hitachi s3400n variable pressure sem has been developed by improving the design of the s3000n vp sem which has been well accepted in the. The hitachi s 3400n sem is a high performance, userfriendly scanning electron microscope with new improvements that allow the best results for a wide range of applications. Hitachi s3500n variable pressure sem university imaging centers. Click on left of gray box on toolbar for normal operation, vacc15 kv and ie10 a. The hitachi s3500n variable pressure scanning electron microscope sem. Download hitachi digital presentation solutions portable lcd data projector brochures, manuals and technical specifications. Improves collection of secondary electron signal for improved low voltage imaging.
Pdf introduction the use of a scanning electron microscope in geological and. Live color cathodoluminescence imaging of geological. Outside of the united states and canada, please contact your closest hitachi dealer. Live color cathodoluminescence imaging of geological specimens in the sem using the hitachi s 3400n sem cathodoluminescence cl occurs when an electron beam strikes a material and causes it to luminesce. Hitachi operating guide plasma television 42edt41a. Purchase cddvd or hard copies of hitachi operating and service manuals online or by phone. Unique vpmode that allows microscopy of wet, oily and nonconductive samples in their natural state without the need of conventional sample preparation. Detecting ironbased pigments on rutheniumcoated ancestral. Hitachi ex2500, ex25005 excavator set of pdf manuals set includes complete technical information, troubleshoot and operain principles manuals, parts catalogs, operator s manual, assembly manual, checks sheets. Always wear gloves when handling anything that goes in the chamberstubs, specimens, sample holders etc. The new hitachi s 3400n variable pressure sem has been developed by improving the design of the s 3000n vp sem which has been well accepted in the world market. Instruction manual for model s3400n scanning electron microscope users operationmaintenance edition please read through this manual carefully. Hitachi s3400n fully automated vp scanning electron. Hitachi ex2500, ex25005 excavator set of pdf manuals set includes complete technical information, troubleshoot and operain principles manuals, parts catalogs, operators manual, assembly manual.
The s3400n has new electron optics, turbomolecular pumping, a new detector, enhanced sample handling and analysis and improved signal processing and display to ensure high quality images can. The video starts at 25x, about 6 mm across the whole field of view, and zooms in to 12000x, about 12. Hitachi s 3400n variable pressure scanning electron microscope with. Our hitachi sem 3400n is equipped with a turbomolecular pump for quick pump down times and reliable high vacuum performance. Home boise state center for materials characterization. Instruction manual 1 this instruction manual and those instruction manuals for relevant accessories may be revised for improvement without prior notice. Ultimate air are distributors for hitachi s wide range of products, service complete with full technical support. The new hitachi s3400n variable pressure sem has been developed by improving the design of the s3000n vp.
Standard operating procedures for hitachi s4800 high resolution sem 11. Ie will drop during the first 30 minutes of usage due to formation of a monolayer of absorbed gas on the tungsten emitter tip. View and download hitachi 32ld4550u service manual online. The specimen chamber needs to go to air to enable the loading of a specimen. The best resolved image of ironbased pigment for the ruthenium. Effective sem analytical techniques for the cathodoluminescence. Peter sandstone is used extensively as a proppant in. Hitachi hd2700 cs corrected scanning transmission electron. We have sem hitachi s3400n in our lab but we could not get clear images for tio2 nanotubes. The boise state center for materials characterization was established by the idaho state board of education in august 2006 to provide a stateoftheart characterization facility in order to attract more. We provide introduction of the s 4300se sem with features and some applications. Open the scanning electron microscope with a key switch, twist from the off position to the start file, the key to on automatically playing files.
Electrochemically mediated nitrate reduction on nanoconfined. Pdf visualization of hydrogels with variablepressure sem. Swave velocities and anisotropy of typical rocks from yunkai. The microscopic features of the resultant nanocomposite were observed under a highresolution transmission electron microscope tem, jeoljem100s. View and download hitachi 9960 instruction manual online. If the sample drops into the chamber, the chamber will have to be disassembled. The hitachi s3400n sem is a high performance, userfriendly scanning electron microscope with new improvements that allow the best results for a wide range of applications. Hitachi s4700 detects the electrons that come from the sample. Fix tightly the sample on the sample holder with the doublesided conductive tape dont use too much tape.
Energy dispersive xray spectroscopy edax the presence of elemental copper was confirmed through eds. We provide introduction of the s4300se sem with features and some applications. Due to operating system limitations on folder depth. Hitachi s3400nii this variable pressure sem with a tungsten filament is capable of imaging and analysis of pristine materials. It is used for observing a physical object by irradiating an electron beam a narrow, focused stream of electrons onto the object by detecting, for example, secondary electrons emitted from the object and reflected electrons emitted when the direction of travel of the irradiating electron beam travelling within the object varies.
Pdf application of peltier cooling device in a variablepressure sem. Specimens were etched in 30% phosphoric acid for 20 seconds followed by thorough rinsing in excess distilled water. Hitachi s3400nii materials research facilities network. View and download hitachi 42edt41a operating manual online. The mk3 coolstage is permanently connected to the hitachi sem, and will be at ambient temperature, as indicated on the control panel the peltier cold head is fragile and must be handled with care for optimal performance. The morphology of the prepared email protected and the spatial distribution of fe within the polymer beads were observed by scanning electron microscopy sem, hitachi s 3400n ii, hitachi, japan. However, due to continuous efforts being made to improve and. Teeth were dried overnight under vacuum and sputter coated with gold. It is used for observing a physical object by irradiating an electron beam a narrow, focused stream of electrons onto the object by detecting, for. We want to know if it is possible to use sem hitachi s 3400n for imaging tio2 nanotubes with. A new analytical chamber provides high take off angle ports for eds and ebsd. Energy dispersive analysis xray spectrometer takes advantage of the. Wait a few minutes until you hear the machine beep 3.
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